List of acquired equipment/instruments within the project:
- Electron transmission microscope TEM
- HPLC chromatography instrument
- Elemental analysis CHNS
- Chemical hood Talassi
- Rotary evaporator LABOROTA 4000+ Rotavac valve control
- Laboratory closet for reagents (2 pieces) (laboratory furniture)
- Glove Box (sealed container with inert atmosphere)
Electron transmission microscope TEM
- Resolution: 0,204nm;
- Acceleration voltage: variable, between 40 – 120kV;
- Zoom factors (for imaging probe): High resolution mode: HC mode 200x – 200.000x, HR mode 4.000x – 600.000x;
- Low mag mode: 50x – 1.000x;
- Small step electron irradiation mode;
- Lens system for irradiation: 2 step condenser lens; variable aperture: 20, 50, 100 si 200µm (4 available aperture numbers)
HPLC chromatography instrument
- Pump: gradient: can work with 4 solvents at low pressure;
- Wide flow range from 0.001 to 10 mL/min with external control in 1µl steps;
- Maximum operating presure: 40MPa=400Bar;
- RS-232 interface control;
- Solvent organiser composed from degasser, low pressure mixer, with accesories and data acquisition interface: maximum flowrate on each channel is 10ml/min;
- Vacuum pump: step by step micropump; >6,2kPa: 400cycles/min; <6,2kPa: 60cycles/min.
- Low pressure gradient mixer: Number of solvents: 4; maximum flowrate on each channel: 50ml/min;
- Column owen: Capacity: a maximum of 2 columns with an external diameter of 12mm 300mm length or 4 columns with 12mm ext. diam. and 125mm length;
- Temperature range: from 10ºC below ambient temperature to 140ºC;
- Diode array detector: stainless steel cell, pressure up to 300 bar (4200psi) optic length of 10 mm; wavelength selection range: 190 – 1150 nm;
- Measuring cell: of 10mm, 10µL, stainless steel for the detector;
- Control software for data acquisition and processing, quantitative determination based on calibration curve;
- HPLC installation kit;
- PC Dual Core, 1GB RAM, 180GB HDD, DWD-RW Dual layer, 17”LCD Color Monitor, keyboard, mouse, Printer Laser A4 Black-white, Windows XP
Elemental analysis CHNS
- Precision and RSD is 0,1%, respectively, maximum sensitivity is 1μg;
- Determination limit: from 0,001 100%;
- Determination sensitivity: from 0 to 100ppm;
- Dynamic combustion temperature is 1150˚C; pyrolysis temperature is 850˚C;
- Owen temperature of cromatographic columns can be set between 40 and 90˚C;
- Detector flow rate (TCD), 200ml/min.
Chemical hood Talassi
- The external bearing structure has been realized with electro-zinc plated steel sheet panels, painted with anticorrosion epoxy powder by transit through heat tunnel at 200°C.
- The suction unit is composed of a tight motor, with polypropylene volute and rotor.
- SAFETY BLOCK safety device automatically assuring the locking of front door at any height in case one or both wire ropes break, as provided for by the regulations.
- “ups and downs” front glazed door with sliding panes
- glazed side walls
- 1 cold water tap
- 1 gas tap
- 1 discharge sink
- 1 lamp for internal lighting
- 1 under cabinet unit with swing doors, extractible
- 1 upper expulsion flange
- Water, gas, electric wiring and discharge internal systems.
Rotary evaporator LABOROTA 4000+ Rotavac valve control
- Equiped with handlift;
- Digital control of: Rotation speed from 20 to 270 rpm, vacuum, bath temperature;
- One heating bath for water and oil 20 °C - 180 °C;
- ROTAVAC Vacuum pump: High suction capacity of 1.7 m³/h, for fastest evacuation; achieves an ultimate vaccum of 9 mbar; rotation speed of 1500 rot/min.
Laboratory closet for reagents (2 pieces) (laboratory furniture)
- Laboratory hazardous substance storage (DN75, EN 14470-1);
- dimensions 1200x1968x615, antiexplosive protection
Glove Box (sealed container with inert atmosphere)
- stainless steel structure, transparent front panel;
- double-gasketed side flange allows easy insertion of process equipment into the work chamber ;
- hermetically sealed chambers;
- includes: fluorescent illuminator 220 VAC 50/60Hz; gloves size 8 P/N 1689-08; accordion sleeve;
- Power Strip; Dual Purge™; Nitro Watch; Controller.
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